不同产地细辛挥发油的GC-MS分析

Analysis of Volatile Oil in Asarum from Various Habitats by GC-MS

摘要:

目的: 采用GC-MS法分析3个不同产地细辛挥发油的化学成分,为其质量评价提供依据。 方法: 采用水蒸气蒸馏法提取细辛挥发油,经正己烷萃取后,采用GC-MS法分析鉴定细辛中主要挥发油的化学成分,并进行比较。 结果: 3个不同产地的细辛挥发油中,共鉴定出18种相同成分,主要包括甲基丁香酚、黄樟醚、爱草醚、3,5-二甲氧基甲苯、α-蒎烯、β-蒎烯、3-蒈烯、优香芹酮、肉豆蔻醚和榄香脂素。 结论: 3个产地细辛挥发油主要成分为甲基丁香酚、黄樟醚、3,5-二甲氧基甲苯等,但各种成分比例存在差异。

Abstract:

Objective: To analyze the chemical components of the essential oil of the Asarum from various habitats and provide scientific basis for its quality control. Method: The essential oil was extracted by water-steam distillation. The relative content of chemical components was identified by GC-MS method. Result: Three batches of A. from various habitats were determined and 18 common characteristic compounds were identified, mainly including the methyl eugenol, safrole, estragole, 3,5-dimethoxy-toluene, α-pinene, β-pinene, 3-carene, eucarvone, myristicin, and elemicin. Conclusion: The essential oils of A. from various habitats are different in the ratio and level of main components.